High pressure, high temperature and low temperature parallel synthesis reactor
Detailed configuration specification: primitive [Schlenk* 12/30ML * twenty-two 0 ℃ * parallel magnetic force * reflux *High pressure reaction below 6MPa * Online vacuum pumping below 0.1MPa * Each tube can be controlled separately *Safety protection * cleanable air chamber * water and air source platform] function item [intelligent heating magnetic stirrer IKA- RCT/domestic magnetic stirrer ]
Main technical parameters:
Superior technical indicators: (indicators superior to similar imported products)
Basic parameters:
1、 Reaction site: /12 bits
2、 reaction container ： 12 bits: 30 ML high voltage Test tube size: diameter 22mm * 156mm ( Single port high pressure test tube )
three 、 Applicable volume: 5-30 ML
four 、 Scope of application: magnetic stirring reaction High temperature and high pressure Reaction, reflux reaction, gas reaction, anhydrous and anaerobic reaction, air bag Hydrogenation reaction Below 6MPa 、 The high vacuum reaction is below - 01MPa, and the gas can be taken now.
5、 Temperature zone: 1 heating Temperature control zone
6、 Heat conduction mode: solid conduction module
7、 Overnight experiment: Yes
8、 Return efficiency: return efficiency ≥ ninety %（ ethanol Loss rate of heating reflux at 80 ℃ for 48h ≤ fifteen %）
9、 Condensation mode I: water free air condensation (suitable for slight reflux of high boiling solvent, B.P. ≥ 80 ℃)
10、 Condensation mode II: external tap water cooling or external ethanol low-temperature circulating liquid (suitable for high-temperature reflux of low boiling solvent, B.P. ≤ 80 ℃)
11. Can low temperature reaction be done: position 12 is equipped with low temperature circulating liquid pump It can react at low temperature within minus 20 ℃.
12、 Connection mode: Silk mouthpiece Lock (new design experience, traditional Silk mouthpiece Connections and clips, The high pressure test tube is connected by the wire mouth, Ensure that the lock is tight and prevent sticking)
