############################################################################### ##此CIF包含接受的数据项目的数据##在IUCrData上发布。它符合##IUCrData作者注释##由IUCrData主持的同行评审## ##结晶信息文件格式的完整详细信息##论文“结晶信息文件(CIF):##《新的晶体学标准档案》,作者S.R.Hall,F.H##艾伦和I.D.布朗【《水晶学报》(1991),A47655-685】## ##核心CIF字典的当前版本可从## ftp://ftp.iucr.org/pub/cif_core.dic。 ## ##软件可免费用于结构的图形显示##CIF价格。有关信息,请参阅CIF软件页面## http://www.iucr.org/resources/cif/software。 ## ##此文件可用于##科学界,只要对数据给予适当的归属#从中获得它的物品## ###############################################################################数据_全局_audit_creation_method“form.cif(2.0版)”_日志数据验证编号?_日记_日期_电子2022-11-09_日记_日期_接受日期2022-11-10_journal_name_full“IUCrData”_2022年日志_日志卷7_日记_第11期_日志_页面_第一个0_日志_页面_最后0_日志_纸张_类别HO_日志_paper_doi 10.1107/S241431462201080X_日记_编辑_代码HB4419_publi_contact_author_name“Md.Belayet Hossain Howlader”_公共联系人作者地址; 化学系拉杰沙希大学拉杰沙希-6205孟加拉国;_publ_contact_author_email”mbhhowlader@yahoo.com'_publ_contact_author_fax“+88-0721-750064”_publ_contact_author_phone'+88-0721-760035'_公共部分标题;4,4'-[辛烷-1,8-二烷基双(氧)]二苯甲酸二乙酯;回路__publ_author_name(发布_作者名称)_公共_作者_地址“苏尔塔娜·沙基拉·汗”;孟加拉国拉杰沙希大学化学系,拉杰沙希-6205;'马里兰州。贝拉耶特·侯赛因·霍拉德;孟加拉国拉杰沙希大学化学系,拉杰沙希-6205;“宫崎骏”;环境保护和研究安全中心,富山大学,3190 Gofuku,富山,930-8555,日本;'马里兰州。Chanmiya Sheikh';理学院应用科学系,日本冈山理工大学;“埃尼奥·赞格兰多”;的里雅斯特大学化学与药学系,意大利;_公共_部分_摘要;中心对称分子几乎是平面的。;数据_I_审计_创建_方法“SHELXL-2019/2”_化学名称系统;4,4'-[辛烷-1,8-二烷基双(氧)]二苯甲酸二乙酯;_化学名称通用?_化学配方‘C26 H34 O6’_化学公式_总和‘C26 H34 O6’_化学配方'C26 H34 O6'_化学配方重量442.53_化学熔点?_空间群晶体系统三斜晶系_space_group_name_H-M_alt“P-1”_space_group_name_Hall“-P 1”回路__空间组符号操作“x,y,z”“-x,-y,-z”_单元格长度a 6.6734(5)_单元格长度_b 9.8044(8)_单元格长度c 10.5156(7)_单元格角度α65.804(5)_单元格_角度_贝塔89.894(6)_单元格角度伽马74.736(5)_单元格_卷601.03(8)_单元格_公式_单位_Z 1_单元格_测量_已使用4497_单元格_测量值_最小值2.44_单元格_测量_最大值25.89_单元格_测量_温度173(2)_exptl_晶体_描述板_exptl_晶体_无色_exptl晶体尺寸最大0.290_exptl晶体尺寸最小值0.210_exptl_crystal_size最小0.060_exptl晶体密度衍射1.223_exptl晶体密度测量?_exptl晶体密度方法?_exptl_晶体_F_000 238_出口_吸收_效率_单位0.086_exptl_absorpt_correction_type多扫描_exptl_absorpt_process_details(导出吸收过程详细信息);(ABSCOR;东,1995年);_exptl_吸收_修正_最小值0.506_exptl _吸收_校正_最大值0.995_衍射环境温度173(2)_衍射源?_衍射_辐射_类型MoK\a_衍射辐射波长0.71075_diffrin_measurement_device_type“里加库R轴快速”_差异测量方法_衍射探测器面积土壤平均值10.000_衍射_反射_编号5815_diffren_refns_av_R等效物0.0299_diffrin_reflns_av_unetI/netI 0.0400_衍射_反射_加热_最小2.139_衍射_反射_热_最大27.461_diffrin_refns_theta完整25.242_衍射_测量_分数_热_最大值0.993_衍射_测量_分数_高度_满0.996_衍射反射极限h最小值-8_衍射反射极限h最大值8_衍射_反射_极限_k最小值-12_衍射反射极限k最大值12_衍射_反射_极限_最小值-13_衍射反射极限最大值12_细化特殊细节?_refns_number_total参考号_总计2739_refns_number_gt 2065号_reflns_threshold_expression“I>2\s(I)”_细分_ls_structure_factor_cef Fsqd_refine_ls_matrix_type已满_refine_ls_R_因子_全部0.0750_精制_ls_R_factor_gt 0.0578_细化_ls_wR_factor_gt 0.1532_细化_ls_wR_factor_ref 0.1637_细化_ls_goodness_of_fit_ref 1.101_细化_限制_全部1.101_refine_ls_number_reflns细化_编号_翻页2739_refine_ls_number_parameters优化_数量_参数146_细化_ls_number_restraints 0_refine_ls_hydrogen_treaction施工_细化_权重_方案计算_细化_权重_详细信息'w=1/[\s^2^(Fo^2^)+(0.0845P)^2^+0.0881P]其中P=_atom_sites_solution_hydrogens地质_atom_sites_solution_primary双重_atom_sites_solution_secondary?_细化_ls_shift/su_max 0.000_精细_偏移/最小0.000_精制密度最大值0.479_细化_密度_最小-0.256_refine_ls_extinction_method无_refine_ls_extinction_cef。回路__原子类型符号_原子类型描述_atom_type_scat_dispersion_real格式_原子类型分类_原子类型类别源“C”“C”0.0033 0.0016“国际表格C卷表4.2.6.8和6.1.1.4”“高”“高”0.0000 0.0000“国际表格C卷表4.2.6.8和6.1.1.4”“O”“O”0.0106 0.0060“国际表格C卷表4.2.6.8和6.1.1.4”_计算数据收集;RAPID-AUTO(里加库,2010年);_计算单元格定义;RAPID-AUTO(里加库,2010);_计算数据还原;RAPID-AUTO(里加库,2010);_计算结构解决方案;SHELXT2014/5页(Sheldrick,2015a);_计算结构定义;SHELXL2019/2型(谢尔德里克,2015b);_计算分子图形;钻石(Brandenburg&Putz,1999);_computing_publication_material?回路__原子站点类型符号_原子站点标签_原子站点分形x_原子站点分形_原子_位_分形_z_原子_站点_U_iso_or_equiv_原子站点地址类型_原子_位_calc_flag_原子站点占用_atom_site监控程序集_原子站点监控程序组O O1 0.50078(18)0.61698(14)0.26687(11)0.0379(3)Uani d 1。O O2-0.15521(19)0.27118(15)0.20288(12)0.0448(4)Uani d 1。O O3-0.13007(18)0.21468(14)0.43290(12)0.0373(3)Uani d 1。C C1 0.9557(3)0.95272(19)0.06471(16)0.0340(4)Uani d 1。H H1A 0.875445 1.023516 0.104138 0.041 Uiso计算值1。H H1B 1.073077 0.875112 0.136554 0.041 Uiso计算值。C C2 0.8136(2)0.86753(19)0.03467(16)0.0331(4)Uani d 1。H H2A 0.696733 0.944785-0.037757 0.040 Uiso计算值。H H2B 0.894056 0.795510-0.003499 0.040 Uiso计算值1。C C3 0.7246(3)0.77505(19)0.16506(16)0.0341(4)Uani d 1。H H3A 0.841692 0.697379 0.237046 0.041 Uiso计算值。H H3B 0.645698 0.847111 0.203703 0.041 Uiso计算值1。C C4 0.5820(3)0.69140(19)0.13702(16)0.0335(4)单位。H H4A 0.466187 0.766566 0.062869 0.040 Uiso计算值1。H H4B 0.660781 0.612463 0.105526 0.040 Uiso计算值1。C C5 0.3632(2)0.53601(18)0.26868(16)0.0306(4)单位。C C6 0.3009(3)0.51230(19)0.15451(16)0.0338(4)单位。H H6 0.354087 0.554669 0.067383 0.041 Uiso计算值。C C7 0.1604(3)0.42621(19)0.16981(17)0.0340(4)单位。H H7 0.118981 0.409221 0.092424 0.041 Uiso计算值1。C C8 0.0786(2)0.36409(18)0.29588(16)0.0301(4)单位。C C9 0.1424(2)0.38832(19)0.40981(16)0.0319(4)Uani d 1。H H9 0.088819 0.346062 0.496787 0.038 Uiso计算值1。C C10 0.2826(3)0.4731(2)0.39638(16)0.0339(4)单位。H H10 0.324872 0.489132 0.474169 0.041 Uiso计算值。C C11-0.0794(2)0.28025(18)0.30258(17)0.0328(4)Uani d 1。C C12-0.2826(3)0.1275(2)0.45125(18)0.0373(4)Uani d 1。H H12A-0.225921 0.035401 0.431134 0.045 Uiso计算值。H H12B-0.413088 0.194284 0.387294 0.045 Uiso计算值。C C13-0.3244(3)0.0773(2)0.60203(19)0.0454(5)Uani d 1。H H13A-0.423756 0.015410 0.620866 0.054 Uiso计算值1。H H13B-0.383525 0.169814 0.619571 0.054 Uiso计算值1。H H13C-0.193089 0.014077 0.663841 0.054 Uiso计算值。回路__原子网站标签_原子_现场_日产_U_11_原子_现场_日产_U_22_原子_地点_尼索_U_33_原子_现场_日产_U_12_原子_现场_日产_U_13_原子_位置_同位素_U_23O1 0.0408(7)0.0495(7).0316(6)-0.0276(6)0.0102(5)-0.0163(5)氧气0.0479(8)0.0588(8)0.0391(7)-0.0288(6)0.0045(5)-0.0236(6)臭氧0.0362(6)0.0433(7)0.0389(7)-0.0228(5)0.0073(5)-0.0170(5)C1 0.0341(9)0.0348(8)0.0357(9)-0.0156(7)0.0060(7)-0.0141(7)C2 0.0322(8)0.0345(8).0354(9)-0.0159(7)0.0063(6)-0.0136(7)C3 0.0339(9)0.0361(9).0342(9)-0.0152(7)0.0060(6)-0.0137(7)C4 0.0327(8)0.0369(9)0.0330(9)-0.0176(7)0.0081(6)-0.0123(7)C5 0.0274(8)0.0324(8).0323(8)-0.0106(6)0.0023(6)-0.0128(6)C6 0.0358(9)0.0394(9)0.0280(8)-0.0151(7)0.0074(6)-0.0135(7)C7 0.0330(9)0.0394(9)0.0134(9)-0.0123(7)0.0022(6)-0.0181(7)C8 0.0273(8)0.0303(8).0335(9)-0.0096(6)0.0021(6)-0.0134(6)C9 0.0309(8)0.0377(9)0.0291(8)-0.0146(7)0.0061(6)-0.0131(6)C10 0.0331(8)0.0438(9)0.0300(8)-0.0167(7)0.0038(6)-0.0171(7)C11 0.0297(8)0.0322(8)0.00380(9)-0.0095(7)0.0039(6)-0.0159(7)C12 0.0331(9)0.0388(9)0.466(10)-0.0186(7)0.0071(7)-0.0196(7)C13 0.0458(11)0.0490(11)0.05(11)-0.0260(9)0.0160(8)-0.0223(8)_地理_特殊_详细信息;所有esd(两个l.s.平面之间二面角的esd除外)使用全协方差矩阵进行估计在估计距离、角度的esd时单独考虑和扭转角;细胞参数中esd之间的相关性仅为当它们由晶体对称性定义时使用。近似(各向同性)细胞esd的处理用于估计涉及l.s.平面的esd。;回路__地理绑定原子站点标签1_地理绑定原子站点标签2_地理绑定站点对称2_地理绑定距离_geom_bond_publ标志O1 C5。1.3581(18) ?O1 C4。1.4421(18) ?氧气C11。1.2105(19) ?臭氧C11。1.3403(19) ?臭氧C12。1.4581(18)?C1 C1 2_775 1.520(3)?C1 C2。1.527(2) ?C1 H1A。0.9900 ?C1 H1B。0.9900 ?C2 C3。1.522(2) ?C2 H2A。0.9900 ?C2 H2B。0.9900 ?C3 C4。1.508(2) ?C3 H3A。0.9900 ?C3 H3B。0.9900 ?C4 H4A。0.9900 ?C4 H4B。0.9900 ?C5 C6。1.396(2) ?C5 C10。1.402(2) ?C6 C7。1.386(2) ?C6 H6。0.9500 ?C7至C8。1.392(2) ?C7 H7。0.9500 ?C8 C9。1.400(2) ?C8 C11。1.484(2) ?C9 C10。1.378(2) ?C9 H9。0.9500 ?C10 H10。0.9500 ?第12段第13段。1.505(2)?C12 H12A。0.9900 ?C12 H12B。0.9900 ?C13 H13A。0.9800 ?C13 H13B。0.9800 ?C13 H13C。0.9800 ?回路__地理角度原子站点标签1_地理角度原子站点标签2_地理角度原子站点标签3_地理角度场地对称1_地理角度场地对称3_地理角度_地理角度ubl标志C5 O1 C4。118.70(12) ?C11 O3 C12。116.54(12) ?C1 C1 C2 2_775。113.30(16) ?C1 C1 H1A 2_775。108.9 ?C2 C1 H1A。108.9 ?C1 C1 H1B 2_775。108.9 ?C2 C1 H1B。108.9 ?H1A C1 H1B。107.7 ?C3 C2 C1。112.54(13) ?C3 C2 H2A。109.1毫米?C1 C2 H2A。109.1毫米?C3 C2 H2B。109.1毫米?C1 C2 H2B。109.1毫米?H2A C2 H2B。107.8 ?C4 C3 C2。113.26(13) ?C4 C3 H3A。108.9 ?C2 C3 H3A。108.9 ?C4 C3 H3B。108.9 ?C2 C3 H3B。108.9 ?H3A C3 H3B。107.7 ?O1 C4 C3。107.07(12) ?O1 C4 H4A。110.3 ?C3 C4 H4A。110.3 ?O1 C4 H4B。110.3 ?C3 C4 H4B。110.3 ?H4A C4 H4B。108.6 ?O1 C5 C6。124.62(14) ?O1 C5 C10。115.71(13) ?C6 C5 C10。119.67(14)?C7 C6 C5。119.21(14) ?C7 C6 H6。120.4 ?C5 C6 H6。120.4 ?C6 C7 C8。121.54(14) ?C6 C7 H7。119.2 ?C8 C7 H7。119.2 ?C7 C8 C9。118.79(14) ?C7 C8 C11。118.64(14) ?C9 C8 C11。122.51(14) ?C10 C9 C8。120.34(14) ?C10 C9 H9。119.8 ?C8 C9 H9。119.8 ?C9 C10 C5。120.44(14) ?C9 C10 H10。119.8 ?C5 C10 H10。119.8 ?氧气C11 O3。123.23(15) ?氧气C11 C8。124.60(15)?O3 C11 C8。112.17(13) ?O3 C12 C13。106.08(14) ?O3 C12 H12A。110.5 ?C13 C12 H12A。110.5 ?O3 C12 H12B。110.5 ?C13 C12 H12B。110.5 ?H12A C12 H12B。108.7 ?C12 C13 H13A。109.5 ?C12 C13 H13B。109.5 ?H13A C13 H13B。109.5 ?C12 C13 H13C。109.5 ?H13A C13 H13C。109.5 ?H13B C13 H13C。109.5 ?回路__地理_扭转_原子_场地_标签1_地理_扭转_原子_场地_标签2_地理_扭转_原子_场地_标签3_地理_扭转_原子_场地_标签_4_地理_扭转_场地_对称_1_地理_扭转_场地_对称_2_地理扭转场地对称3_地理_扭转_场地_对称_4_地理扭转_地理_扭转_取消标记C1 C1 C2 C3 2_775-179.35(16) ?C1 C2 C3 C4。179.44(14) ?C5 O1 C4 C3。178.54(13) ?C2 C3 C4 O1-176.76(13) ?C4 O1 C5 C6。3.3(2) ?C4 O1 C5 C10-176.98(13) ?O1 C5 C6 C7。179.46(15) ?C10 C5 C6 C7-0.2(2) ?C5 C6 C7 C8。0.6(2) ?C6 C7 C8 C9-0.7(2) ?C6 C7 C8 C11。176.84(14) ?C7 C8 C9 C10。0.4(2) ?C11 C8 C9 C10-177.00(15) ?C8 C9 C10 C5-0.1(2) ?O1 C5 C10 C9-179.73(14)?C6 C5 C10 C9。0.0(2) ?C12 O3 C11 O2。0.8(2) ?C12 O3 C11 C8-179.24(13) ?C7 C8 C11 O2-5.7(2) ?C9 C8 C11氧气。171.73(16) ?C7 C8 C11 O3。174.33(13) ?C9 C8 C11 O3-8.2(2) ?C11 O3 C12 C13-175.71(14) ?回路__地理_hbond_atom_site_label_D_地理_hbond_atom_site_label_H_地理_绑定_原子_站点_标签_A_地理_邦_场地_对称_A_地理_绑定_距离_DH_地理_绑定_距离_HA_地理_绑定_距离_DA_geom_hbond_angle_DHAC3 H3A Cg1 1_655 0.99 2.89 3.728(2)143C12 H12B Cg1 1_455 0.99 2.82 3.744(2)155_货架空间组注释;这种shelxl细化所采用的对称性是唯一定义的由以下循环执行,该循环应始终用作对称信息优先于上述空间组名称。它们仅用作注释。;_货架_估计_吸收T_最小值0.976_货架_估计_吸收T_max 0.995_shelx _ hkl文件;0 0 -1 29.96 0.410 0 -1 32.95 0.290 0 2 129.72 2.120 0 2 134.18 1.620 0 -2 134.26 2.180 0 -2 139.10 1.660 0 3 81.17 1.520 0 3 75.09 0.870 0-3 76.40 1.280 0 4 18.72 0.540 0 -4 18.51 0.500 0 5 76.97 1.880 0 -5 77.54 1.800 0 6 45.91 1.450 0 -6 47.39 1.420 0 7 192.97 4.270 0 -7 199.29 4.320 0 8 34.29 1.230 0 -8 35.14 1.550 0-9 87.94 2.920 0 -10 0.44 0.770 0 -11 1.58 0.660 0 -12 -0.29 0.640 1-11 2.19 0.730 1 -10 -0.17 0.800 -1 10 0.44 0.590 1 -9 8.33 1.110 -1 9 6.51 0.760 1 -8 48.24 1.900 -1 8 45.87 1.520 1 -7 15.77 1.020 -1 7 14.71 0.780 1 -6 7.64 0.690 1 -6 5.56 0.190 -1 6 7.26 0.510 -1 6 5.66 0.160 1 -5 61.91 1.530 1 -5 57.30 0.890 -1 5 61.25 1.630 -1 5 57.38 0.860 1 -4 137.47 2.750 1 -4 131.64 2.040 -1 4 137.46 2.880 -1 4 132.96 1.970 1 -3 77.64 1.500 -1 3 81.19 1.620-1 3 76.38 1.090 1 -2 47.73 0.920 -1 2 45.40 0.760 -1 2 46.25 0.640 1 -1 85.61 1.240 1 -1 93.46 1.250 -1 1 86.88 1.340 -1 1 91.47 1.210 1 1 5.75 0.120 -1 -1 5.71 0.110 1 2 4479.05 159.530-1-2 4694.22 166.790 1 3 40.64 0.510 -1 -3 44.55 0.760 -1 -3 45.24 0.520-1-4 168.91 3.270 -1 -4 158.53 2.130 -1 -4 169.45 2.220 -1 -5 5.23 0.550 -1 -6 1.36 0.300 -1 -7 212.80 4.570 -1 -8 -0.24 0.360 -1 -9 276.79 6.720 -1 -10 18.28 0.980 -1 -11 10.82 0.940 -1 -12 7.64 0.980 2 -11 3.47 0.910 -2 11 5.54 1.000 2 -10 2.35 1.090 -2 10 2.18 0.740 2 -9 0.16 0.440 -2 9 0.02 0.500 2 -8 0.28 0.630 -2 8 -0.67 0.680 2 -7 20.35 1.210 2 -7 14.48 0.440 -2 7 19.80 1.360 2 -6 160.56 4.060 2-6 142.94 2.700 -2 6 166.41 4.400 2 -5 17.00 0.850 2 -5 14.15 0.490 -2 5 18.56 0.930 2 -4 38.71 1.090 2 -4 34.71 0.790 -2 4 36.29 0.900 -2 4 34.80 0.670 2 -3 1.11 0.310 2 -3 0.38 0.190-2 3 0.41 0.210 -2 3 0.70 0.170 2 -2 31.59 0.630 -2 2 33.50 0.640-2 2 32.88 0.650 2 -1 38.44 0.590 -2 1 40.32 0.620 2 0 0.55 0.110 -2 0 0.85 0.190 2 1 91.63 1.290 -2 -1 86.35 1.210 2 2 45.18 0.730 -2 -2 50.56 0.810 2 3 467.36 8.890 -2 -3 518.09 9.690 2 4 13.02 0.320 -2 -4 12.42 0.250 -2 -5 101.74 1.950 -2 -5 106.18 1.500 -2 -6 64.22 1.380 -2 -6 61.67 0.830 -2 -7 9.83 0.520 -2 -8 124.61 3.250 -2 -9 237.44 6.370 -2 -10 1.17 0.550 -2 -11 17.69 1.110 -2 -12 0.81 0.630-2-13 10.59 1.740 -3 10 7.12 1.550 3 -9 -0.24 0.470 -3 9 0.17 0.500 3 -8 0.82 0.720 3 -8 0.03 0.240 -3 8 0.95 0.790 -3 8 0.16 0.180 3 -7 0.74 0.600 3 -7 -0.19 0.270 -3 7 0.79 0.660-3 7 0.17 0.150 3 -6 6.36 0.820 3 -6 4.38 0.360 -3 6 5.49 0.600-3 6 5.14 0.370 3 -5 255.05 5.730 3 -5 244.13 4.990 -3 5 258.07 6.460 -3 5 245.95 5.030 3 -4 19.01 0.660 -3 4 21.74 0.990 -3 4 18.68 0.550 3 -3 100.19 1.930 -3 3 97.99 2.200 -3 3 101.03 1.900 3 -2 36.18 0.870 -3 2 34.02 0.910 -3 2 35.08 0.830 3 -1 33.91 0.660 -3 1 36.21 0.860 3 0 11.23 0.340 -3 0 10.95 0.330 3 1 255.91 4.580 -3 -1 239.25 4.100 3 2 442.78 8.560 -3 -2 407.01 7.790 3 3 -0.61 0.240-3-3-0.10 0.210 3 4 165.52 2.880 -3 -4 158.86 2.700 3 5 10.00 0.480 -3 -5 9.70 0.320 3 6 5.32 0.340 -3 -6 5.29 0.260 -3 -7 34.22 1.260 -3 -7 31.74 0.590 -3 -8 0.78 0.570 -3 -8 0.85 0.100-3-8 0.32 0.110 -3 -9 -0.03 0.550 -3 -10 27.18 1.620 -3 -11 -0.60 0.500-3-12 0.84 0.960 -3 -13 10.08 1.660 -4 9 0.76 1.070 4 -8 0.66 0.430 -4 8 1.45 0.650 -4 8 0.80 0.250 4 -7 0.19 0.350 -4 7 0.11 0.700 -4 7 0.06 0.260 4 -6 1.55 0.340 -4 6 1.47 0.510 -4 6 0.88 0.350 4 -5 6.99 0.510 -4 5 8.71 0.940 -4 5 7.59 0.420 4 -4 0.52 0.310 -4 4 0.35 0.520 -4 4 0.90 0.290 4 -3 395.41 8.850 -4 3 421.14 9.950 -4 3 432.04 9.450 4 -2 1.69 0.350 -4 2 2.15 0.420-4 2 1.94 0.330 4 -1 13.11 0.450 -4 1 12.28 0.420 4 0 9.24 0.580 -4 0 8.39 0.380 4 1 15.01 0.460 -4 -1 14.71 0.440 4 2 102.04 2.040 -4 -2 99.81 1.960 4 3 138.87 2.610 -4 -3 130.01 2.240 4 4 398.17 8.170 -4 -4 400.53 8.090 4 5 27.41 0.760 -4 -5 26.40 0.710 4 6 68.22 1.380 -4 -6 74.69 1.400 4 7 44.00 0.950 -4 -7 45.06 0.920 -4 -8 6.88 0.500 -4 -8 2.15 0.250 -4 -9 0.94 0.600 -4 -9 0.28 0.170 -4 -10 4.04 0.970 -4 -11 11.83 0.890 -4 -12 2.24 1.090 -4 -13 10.14 1.650 -5 8 2.33 1.250 5 -7 0.49 0.380 -5 7 0.93 0.580 -5 7 0.40 0.310 5 -6 0.36 0.340 -5 6 0.98 0.740 -5 6 -0.02 0.280 5 -5 0.03 0.360 -5 5 0.35 0.410 -5 5 0.30 0.280 5 -4 1.08 0.410-5 4 1.17 0.410 -5 4 1.10 0.320 5 -3 0.47 0.340 -5 3 0.07 0.310 -5 3 0.13 0.310 5 -2 2.11 0.420 -5 2 2.00 0.500 -5 2 2.34 0.400 5 -1 4.84 0.330 -5 1 5.38 0.480 5 0 0.83 0.400-5 0 1.58 0.400 5 1 26.74 0.930 -5 -1 27.50 0.700 5 2 1.16 0.280-5-2 2.18 0.430 5 3 22.46 0.860 -5 -3 20.77 0.580 5 4 52.73 1.310 -5 -4 49.86 1.010 5 5 2.94 0.390 -5 -5 2.10 0.370 5 6 130.29 2.720 -5 -6 134.44 2.710 5 7 2.67 0.360 -5 -7 2.35 0.320 5 8 3.00 0.360 -5 -8 3.01 0.320 -5 -9 0.53 0.620 -5 -9 0.18 0.200 -5 -10 22.12 1.420 -5 -10 13.93 0.470 -5 -11 -0.01 0.470 -5 -11 -0.03 0.120 -5 -11 0.16 0.130 -5 -12 9.76 1.450 -5 -13 14.48 1.220 6 -7 0.09 0.440-6 7 0.83 1.020 -6 7 0.56 0.490 6 -6 0.64 0.500 -6 6 1.94 0.950 -6 6 0.85 0.400 6 -5 1.83 0.570 -6 5 4.60 0.950 -6 5 2.47 0.450 6 -4 -0.02 0.400 -6 4 0.83 0.620 -6 4 0.04 0.320 6-3 7.07 0.710 -6 3 7.67 0.620 -6 3 7.31 0.550 6 -2 -0.16 0.420-6 2 0.03 0.480 -6 2 -0.47 0.400 6 -1 1.13 0.460 -6 1 0.87 0.300 -6 1 -0.12 0.410 6 0 14.39 0.820 -6 0 14.90 0.760 6 1 8.95 0.640 -6 -1 8.37 0.660 6 2 16.70 0.830 -6 -2 17.52 0.830 6 3 6.30 0.400 -6 -3 6.93 0.410 6 4 0.49 0.380 -6 -4 0.08 0.370 6 5 42.77 1.260 -6 -5 42.98 1.220 6 6 33.68 1.120 -6 -6 36.41 1.110 6 7 8.93 0.620 -6 -7 8.83 0.400 6 8 0.22 0.300 -6 -8 -0.24 0.270 6 9 1.66 0.510 -6 -9 1.23 0.340 -6 -10 77.36 2.690 -6 -10 42.16 1.440 -6 -11 1.88 0.580 -6 -11 0.64 0.260 -6 -12 11.80 1.590 -6 -13 4.71 1.370 7 -6 6.82 0.930 -7 6 10.99 1.650 -7 6 6.46 0.790 7-5 0.40 0.550 -7 5 0.73 0.900 -7 5 0.58 0.280 7 -4 3.35 0.480-7 4 4.49 0.700 -7 4 3.68 0.590 7 -3 1.37 0.380 -7 3 0.76 0.500 -7 3 1.50 0.310 7 -2 4.20 0.710 -7 2 4.45 0.550 -7 2 4.23 0.550 7 -1 -0.08 0.450 -7 1 -0.34 0.490 -7 1 0.38 0.410 7 0 4.69 0.760 -7 0 5.58 0.670 7 1 69.47 2.050 -7 -1 67.37 1.940 7 2 0.46 0.480 -7 -2 0.22 0.290 7 3 0.29 0.470 -7 -3 -0.74 0.450 7 4 3.76 0.400 -7 -4 3.72 0.600 7 5 0.41 0.490 -7 -5 0.87 0.450 7 6 10.30 0.790 -7 -6 8.85 0.730 7 7 4.25 0.410 -7 -7 4.81 0.570 7 8 3.77 0.590 -7 -8 4.17 0.360 7 9 2.64 0.510 -7 -9 2.25 0.450 7 10 0.61 0.430 -7 -10 0.71 0.340 -7 -11 1.31 0.880-7-11 0.32 0.320 -7 -12 17.08 1.210 -7 -13 14.12 1.900 8 -5 2.28 0.790-8 5 3.13 1.270 -8 5 1.95 0.650 8 -4 0.44 0.390 -8 4 -0.10 0.570 -8 4 0.47 0.320 8 -3 1.79 0.470 -8 3 1.12 0.930 -8 3 1.26 0.560 8 -2 0.43 0.650 -8 2 1.17 0.760 -8 2 1.04 0.500 8 -1 2.76 0.740 -8 1 1.70 0.850 -8 1 2.75 0.690 8 0 13.04 1.100 -8 0 13.68 1.000 8 1 32.78 1.180 -8 -1 34.73 1.450 8 2 14.90 0.780 -8 -2 15.43 0.760 8 3 34.23 1.160 -8 -3 36.28 1.470 8 4 46.85 1.810-8-4 49.14 1.780 8 5 15.66 0.770 -8 -5 16.97 1.030 8 6 0.24 0.500 -8 -6 -0.50 0.470 8 7 0.03 0.480 -8 -7 -0.34 0.450 8 8 6.17 0.520 -8 -8 6.09 0.700 8 9 0.29 0.510 -8 -9 0.72 0.440 8 10 4.34 0.690 -8 -10 4.41 0.620 8 11 0.05 0.450 -8 -11 0.45 0.380-8-12 1.53 1.010 -8 -12 0.61 0.410 -8 -13 5.95 1.540 9 -4 0.76 0.500 -9 4 0.67 1.120 -9 4 1.00 0.640 9 -3 0.18 0.470 -9 3 0.88 0.960 -9 3 0.90 0.570 9 -2 -0.49 0.790 -9 2 0.98 0.610 -9 2 2.07 0.660 9 -1 -0.70 0.650 -9 1 0.40 0.440 -9 1 0.39 0.550 9 0 4.15 0.940 -9 0 3.49 0.610 -9 0 4.88 0.870 9 1 -0.09 0.400 -9 -1 -0.37 0.580 9 2 37.46 1.850 -9 -2 37.91 1.290 9 3 21.84 1.030-9-3 23.17 1.320 9 4 1.98 0.530 -9 -4 2.32 0.750 9 5 7.10 0.970 -9 -5 6.74 0.610 9 6 10.54 0.720 -9 -6 11.36 1.010 9 7 15.63 0.820 -9 -7 16.00 1.120 9 8 2.61 0.750 -9 -8 2.08 0.430 9 9 13.58 1.160 -9 -9 14.33 1.070 9 10 20.25 1.370 -9 -10 21.46 1.270 9 11 2.31 0.680 -9 -11 1.54 0.590 9 12 5.59 0.860 -9 -12 4.15 0.730 10 -2 -0.77 0.710 -10 2 0.27 0.880 -10 2 0.24 0.590 10 -1 3.16 1.030 -10 1 2.88 1.110 -10 1 3.07 0.930 10 0 0.09 0.440 -10 0 -0.04 0.470 -10 0 0.10 0.590 10 1 -0.21 0.700 -10 -1 0.05 0.590 10 2 -0.18 0.770 -10 -2 -0.51 0.470 10 3 5.32 1.070 -10 -3 5.41 0.990 10 4 0.38 0.770 -10 -4 0.99 0.730 10 5 0.86 0.500 -10 -5 0.69 0.440 10 6 9.68 1.160 -10 -6 9.62 0.720 10 7 21.90 1.490 -10 -7 20.57 1.400 10 8 5.53 0.690 -10 -8 5.50 0.900 10 9 1.59 0.550 -10 -9 2.25 0.480 10 10 2.39 0.820 -10 -10 2.44 0.710 10 11 5.65 0.980-10-11 5.41 0.870 11 0 1.22 0.670 -11 0 1.89 0.720 -11 0 1.40 0.900 11 1 1.71 1.090 -11 -1 2.51 0.710 -11 -1 2.42 0.930 11 2 0.33 0.740 11 2 0.20 0.750 -11 -2 -0.19 0.410 11 3 0.05 0.760 -11 -3 0.02 0.720 11 4 10.24 1.500 -11 -4 11.11 0.950 11 5 11.90 1.490 -11 -5 12.07 0.960 11 6 4.54 0.770 -11 -6 4.79 1.080 11 7 0.95 0.960 -11 -7 1.57 0.560 11 8 2.83 1.040 -11 -8 2.42 0.600 11 9 8.25 0.860 -11 -9 9.40 1.190 11 10 5.72 1.120 -11 -10 6.16 0.660 12 4 8.80 1.560-12-4 8.13 0.870 12 5 8.12 1.560 -12 -5 9.55 1.340 12 6 14.20 1.740 -12 -6 12.93 1.500 12 7 18.14 1.350 -12 -7 19.82 1.630 12 8 0.96 0.930 -12 -8 0.09 0.771 -11 -9 0.97 0.82-1 11 9 1.50 0.581-11-8 2.31 0.59-1 11 8 2.00 0.651 -11 -7 3.73 0.98-1 11 7 1.62 1.081-11-6 3.36 0.98-1 11 6 2.20 0.711 -11 -5 0.78 0.92-1 11 5 1.70 0.991 -11 -4 3.82 1.06-1 11 4 1.88 1.151 -11 -3 6.63 0.87-1 11 3 7.69 1.39-1 11 2 0.45 0.92-1 11 1 1.10 1.021 -10 -11 2.80 0.77-1 10 11 3.08 0.591 -10 -10 1.03 0.65-1 10 10 0.17 0.731 -10 -9 5.80 0.64-1 10 9 5.34 1.021 -10 -8 1.33 0.82-1 10 8 3.40 0.881 -10 -7 1.42 0.77-1 10 7 1.32 0.841 -10 -6 13.45 0.88-1 10 6 13.04 0.931 -10 -5 14.50 0.92-1 10 5 13.77 1.451 -10 -4 4.56 1.04-1 10 4 4.44 1.081 -10 -3 4.30 1.01-1 10 3 2.26 1.041 -10 -2 9.78 0.84-1 10 2 9.31 1.331 -10 -1 11.68 1.30-1 10 1 10.87 1.421 -10 0 0.07 0.931 -10 0 -0.03 0.47-1 10 0 0.71 0.521 -10 1 0.84 0.941 -10 1 -0.02 0.69-1 10 -1 0.07 0.791-9-12 0.36 0.47-1 9 12 0.30 0.541 -9 -11 -0.30 0.45-1 9 11 0.18 0.511 -9 -10 1.51 0.63-1 9 10 1.31 0.701 -9 -9 0.43 0.35-1 9 9 0.40 0.381 -9 -8 -0.35 0.57-1 9 8 -0.41 0.381 -9 -7 2.08 0.67-1 9 7 0.93 0.451 -9 -6 1.16 0.62-1 9 6 -0.28 0.661 -9 -5 3.64 0.80-1 9 5 3.52 0.571 -9 -4 1.88 0.76-1 9 4 1.78 0.851 -9 -3 8.03 1.05-1 9 3 8.31 1.051 -9 -2 20.84 1.39-1 9 2 18.15 1.411 -9 -1 6.21 0.97-1 9 1 5.79 1.061 -9 0 1.65 0.77-1 9 0 1.61 0.541 -9 1 0.45 0.931 -9 1 0.19 0.45-1 9 -1 2.34 0.761 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14.98 1.001 -7 -4 1.11 0.47-1 7 4 -0.12 0.541 -7 -3 1.88 0.37-1 7 3 1.69 0.601 -7 -2 2.87 0.62-1 7 2 3.37 0.461 -7 -1 -0.24 0.49-1 7 1 -0.11 0.501 -7 0 0.15 0.50-1 7 0 0.21 0.501-7 1 0.51 0.411 -7 1 0.42 0.54-1 7 -1 1.13 0.581 -7 2 1.36 0.501 -7 2 0.73 0.33-1 7 -2 1.95 0.611 -7 3 0.07 0.791 -7 3 0.18 0.45-1 7 -3 1.01 0.541 -7 4 -0.06 0.471 -7 4 0.41 0.41-1 7-4-0.33 0.501 -7 5 -0.23 0.931 -7 5 0.09 0.48-1 7 -5 -0.76 0.561-7 6 0.53 1.041 -7 6 0.11 0.47-1 7 -6 0.33 0.551 -6 -13 4.07 0.931 -6 -12 10.80 1.611 -6 -11 9.10 1.23-1 6 11 3.43 0.601 -6 -10 0.29 0.29-1 6 10 0.58 0.341 -6 -9 1.24 0.37-1 6 9 1.46 0.401 -6 -8 12.66 0.49-1 6 8 12.61 0.721 -6 -7 17.11 0.58-1 6 7 16.94 0.841 -6 -6 1.60 0.41-1 6 6 1.36 0.461 -6 -5 130.00 2.91-1 6 5 133.69 3.061 -6 -4 55.51 1.47-1 6 4 56.81 1.581 -6 -3 9.59 0.64-1 6 3 8.52 0.461-6-2 7.36 0.42-1 6 2 6.25 0.431 -6 -1 2.34 0.47-1 6 1 0.98 0.321 -6 0 0.14 0.26-1 6 0 0.05 0.261 -6 1 6.39 0.69-1 6 -1 6.15 0.671 -6 2 77.58 2.511 -6 2 80.99 2.171 -6 3 6.77 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1.00 0.631 -5 7 0.47 0.36-1 5 -7 0.63 0.451 -5 8 0.51 1.041 -4 -13 1.46 0.771 -4 -12 1.64 1.051 -4 -11 4.51 1.191-4-9 144.05 4.09-1 4 9 112.09 2.241 -4 -8 0.94 0.29-1 4 8 1.14 0.241 -4 -7 2.00 0.26-1 4 7 1.64 0.261 -4 -6 42.48 0.94-1 4 6 42.10 1.001 -4 -5 3.33 0.35-1 4 5 3.05 0.331 -4 -4 233.24 4.52-1 4 215.64 4.221 -4 -3 51.86 1.00-1 4 3 54.12 1.271 -4 -2 0.86 0.24-1 4 2 1.58 0.261 -4 -1 25.28 0.86-1 4 1 25.90 0.861 -4 0 2.28 0.29-1 4 0 2.47 0.431 -4 1 4.69 0.30-1 4 -1 4.78 0.311 -4 2 5.18 0.591 -4 2 4.78 0.30-1 4 -2 4.65 0.421 -4 3 9.18 0.551 -4 3 8.45 0.53-1 4 -3 9.76 0.611 -4 4 9.10 0.591 -4 4 8.94 0.50-1 4 -4 8.10 0.561 -4 5 94.64 2.481 -4 5 86.60 2.07-1 4 -5 77.59 2.111 -4 6 16.40 0.981 -4 6 13.64 0.66-1 4 -6 12.96 0.721 -4 7 -0.68 0.811-4 7 0.30 0.27-1 4 -7 0.11 0.321 -4 8 -0.21 0.561 -4 8 0.22 0.34-1 4 -8 0.17 0.401 -4 9 -1.42 1.221 -3 -13 6.53 1.071 -3 -12 0.15 0.901 -3 -11 3.23 1.031 -3 -10 173.67 5.141 -3 -9 19.59 1.371-3-8 231.36 5.741 -3 -8 199.48 3.49-1 3 8 193.23 3.501 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2.971 1 4 59.05 1.31-1-1-4 56.39 1.02-1 -1 -4 56.53 0.841 1 5 3.27 0.33-1 -1 -5 3.67 0.45-1 -1 -5 3.75 0.171 1 6 30.22 1.09-1 -1 -6 32.80 1.07-1 -1 -6 32.72 0.521 1 7 3.28 0.62-1 -1 -7 2.92 0.38-1 -1 -7 2.97 0.13-1 -1 -7 2.85 0.181 1 8 0.72 0.44-1 -1 -8 1.20 0.59-1 -1 -9 38.68 1.73-1 -1 -10 25.10 1.60-1 -1 -11 0.69 0.56-1 -1 -12 4.30 1.321 2 -11 4.49 1.331 2 -10 -0.82 0.601 2 -9 3.07 0.97-1 -2 9 2.49 1.061 2 -8 2.60 0.84-1-2 8 2.95 0.881 2 -7 7.37 0.84-1 -2 7 6.31 0.921 2 -6 4.48 0.45-1 -2 6 5.18 0.74-1 -2 6 4.26 0.211 2 -5 41.27 1.23-1 -2 5 41.55 1.33-1 -2 5 38.51 0.651 2 -4 1419.61 39.791 2 -4 1401.17 37.11-1-2 4 1386.06 38.65-1 -2 4 1363.08 35.491 2 -3 2.14 0.231 2 -3 1.94 0.26-1-2 3 2.19 0.39-1 -2 3 2.01 0.221 2 -2 84.54 1.531 2 -2 82.05 1.47-1 -2 2 84.64 1.59-1 -2 2 81.89 1.391 2 -1 2.85 0.221 2 -1 2.87 0.27-1 -2 1 2.94 0.21-1 -2 1 2.48 0.161 2 0 19.42 0.50-1 -2 0 19.28 0.481 2 1 479.45 9.30-1 -2 -1 483.48 9.35-1 -2 -2 368.99 6.74-1 -2 -3 526.99 10.56-1 -2 -3 530.03 10.48-1 -2 -4 76.21 1.38-1 -2 -4 70.66 1.10-1 -2 -5 97.79 2.02-1 -2 -5 96.97 1.57-1 -2 -5 97.78 1.57-1 -2 -6 103.09 2.30-1-2-6 97.73 1.50-1 -2 -6 95.17 1.50-1 -2 -7 0.54 0.29-1 -2 -7 0.57 0.13-1 -2 -7 0.69 0.15-1 -2 -8 -0.04 0.32-1 -2 -8 0.28 0.09-1 -2 -8 0.25 0.09-1 -2 -9 1.25 0.45-1 -2 -10 4.68 0.62-1 -2 -11 0.30 0.50-1-2-12 8.60 0.931 3 -10 0.02 0.55-1 -3 10 -0.29 0.931 3 -9 3.52 1.06-1-3 9 3.49 1.13-1 -3 8 4.15 0.97-1 -3 8 1.87 0.161 3 -7 1.99 0.73-1 -3 7 2.04 0.85-1 -3 7 1.90 0.181 3 -6 1.12 0.501 3 -6 0.07 0.21-1 -3 6 0.54 0.36-1 -3 6 0.24 0.181 3 -5 2.02 0.531 3 -5 1.98 0.29-1 -3 5 2.48 0.591 3 -4 0.31 0.231 3 -4 0.16 0.28-1 -3 4 0.10 0.26-1 -3 4 0.54 0.231 3 -3 1.61 0.251 3 -3 2.01 0.29-1 -3 3 2.40 0.41-1 -3 3 2.14 0.281 3 -2 265.95 5.21-1 -3 2 273.60 5.53-1-3 2 271.39 5.181 3 -1 51.87 0.95-1 -3 1 54.79 1.03-1 -3 1 53.84 1.101 3 0 12.94 0.38-1 -3 0 13.34 0.521 3 1 0.72 0.18-1 -3 -1 0.77 0.281 3 2 148.20 2.54-1 -3 -2 153.64 2.761 3 3 32.76 0.66-1-3-3 33.42 0.60-1 -3 -4 7.53 0.30-1 -3 -5 305.15 6.15-1 -3 -5 303.20 5.58-1-3-6 28.97 0.75-1 -3 -6 31.63 0.64-1 -3 -7 2.17 0.52-1 -3 -7 1.99 0.17-1 -3 -7 2.05 0.21-1 -3 -8 3.52 0.64-1 -3 -8 2.79 0.22-1 -3 -8 2.88 0.20-1 -3 -9 17.81 1.16-1 -3 -9 13.94 0.30-1 -3 -9 13.95 0.28-1 -3 -10 0.86 0.45-1 -3 -11 4.70 0.70-1 -3 -12 13.93 1.04-1 -3 -13 0.74 1.04-1 -4 9 11.15 1.66-1 -4 8 1.62 0.92-1 -4 8 0.38 0.231 4 -7 4.38 0.62-1 -4 7 5.01 1.041 4 -6 2.92 0.471 4 -6 2.30 0.47-1 -4 6 3.00 0.52-1-4 6 1.61 0.341 4 -5 2.34 0.36-1 -4 5 3.08 0.70-1 -4 5 2.50 0.341 4 -4 12.64 0.58-1 -4 4 14.41 0.88-1 -4 4 13.06 0.551 4 -3 1.48 0.32-1 -4 3 0.98 0.41-1 -4 3 1.32 0.291 4 -2 41.39 0.88-1-4 2 43.39 1.12-1 -4 2 44.09 0.881 4 -1 64.74 1.51-1 -4 1 63.45 1.19-1-4 1 65.88 1.451 4 0 88.91 1.93-1 -4 0 89.62 1.631 4 1 16.17 0.50-1 -4 -1 15.70 0.641 4 2 49.63 1.23-1 -4 -2 47.37 0.931 4 3 16.15 0.48-1 -4 -3 18.16 0.661 4 4 31.25 0.91-1 -4 -4 33.06 0.881 4 5 219.35 4.40-1 -4 -5 228.36 4.33-1 -4 -6 3.51 0.24-1 -4 -7 10.81 0.74-1 -4 -7 10.25 0.36-1 -4 -8 7.36 0.74-1 -4 -8 6.06 0.28-1 -4 -8 6.03 0.26-1 -4 -9 80.02 2.43-1 -4 -9 77.30 1.45-1 -4 -10 2.94 0.74-1 -4 -10 1.04 0.16-1-4-11 7.89 0.80-1 -4 -12 7.78 1.32-1 -4 -13 1.03 1.08-1 -5 9 -0.16 0.63-1 -5 8 0.89 0.661 5 -7 17.32 0.93-1 -5 7 13.28 0.761 5 -6 0.83 0.41-1 -5 6 0.85 0.52-1 -5 6 1.27 0.291 5 -5 3.57 0.50-1-5 5 4.88 0.85-1 -5 5 3.61 0.381 5 -4 13.39 0.72-1 -5 4 15.09 1.02-1-5 4 13.22 0.571 5 -3 7.95 0.62-1 -5 3 9.15 0.74-1 -5 3 9.76 0.561 5 -2 21.55 0.85-1 -5 2 21.95 0.90-1 -5 2 21.94 0.761 5 -1 0.95 0.37-1 -5 1 0.69 0.34-1 -5 1 0.95 0.371 5 0 111.87 2.19-1 -5 0 116.53 2.391 5 1 16.79 0.58-1 -5 -1 18.47 0.771 5 2 2.00 0.50-1 -5 -2 1.94 0.481 5 3 18.97 0.84-1 -5 -3 18.24 0.561 5 4 0.45 0.34-1 -5 -4 -0.29 0.201 5 5 9.42 0.40-1 -5 -5 10.38 0.381 5 6 42.46 1.14-1-5-6 43.57 1.06-1 -5 -7 0.92 0.29-1 -5 -8 5.23 0.70-1 -5 -8 5.02 0.40-1 -5 -9 10.61 0.93-1 -5 -9 7.40 0.39-1 -5 -10 3.02 0.84-1 -5 -10 2.07 0.32-1 -5 -10 2.64 0.34-1 -5 -11 27.33 0.59-1 -5 -11 26.81 0.59-1-5-12 14.08 1.51-1 -5 -13 4.20 1.28-1 -6 8 8.70 1.631 6 -7 1.30 0.64-1-6 7 1.87 0.66-1 -6 7 0.23 0.371 6 -6 4.35 0.67-1 -6 6 7.35 1.19-1 -6 6 4.04 0.631 6 -5 6.57 0.67-1 -6 5 7.52 0.75-1 -6 5 6.38 0.541 6 -4 3.71 0.61-1 -6 4 4.25 0.83-1 -6 4 4.13 0.451 6 -3 8.36 0.75-1 -6 3 9.85 0.87-1 -6 3 9.32 0.581 6 -2 1.02 0.47-1 -6 2 0.94 0.49-1 -6 2 0.89 0.421 6 -1 3.52 0.36-1 -6 1 3.56 0.53-1 -6 1 3.47 0.331 6 0 70.46 1.55-1 -6 0 67.65 1.411 6 1 32.16 0.87-1-6-1 35.14 0.901 6 2 243.08 4.99-1 -6 -2 251.29 5.251 6 3 108.54 2.52-1 -6 -3 101.24 1.971 6 4 13.65 0.75-1 -6 -4 12.84 0.671 6 5 7.69 0.60-1 -6 -5 6.61 0.521 6 6 0.05 0.21-1 -6 -6 -0.10 0.171 6 7 0.64 0.36-1 -6 -7 0.07 0.331 6 8 4.35 0.51-1 -6 -8 3.72 0.41-1-6-9 0.73 0.65-1 -6 -9 0.63 0.39-1 -6 -10 0.26 0.66-1 -6 -10 0.38 0.28-1 -6 -11 3.15 0.58-1 -6 -11 1.52 0.36-1 -6 -11 1.33 0.30-1 -6 -12 6.95 1.28-1 -6 -13 1.85 0.731 7 -7 0.64 0.78-1 -7 7 2.02 1.15-1 -7 7 0.90 0.581 7 -6 0.15 0.53-1 -7 6 0.64 0.93-1 -7 6 0.45 0.401 7 -5 3.85 0.71-1 -7 5 4.65 1.12-1 -7 5 2.94 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4.51 0.79-6 -6 5 5.25 0.80-6 -6 4 8.79 0.90-6 -6 4 9.17 0.94-6 -6 3 4.27 0.76-6 -6 3 3.35 0.78-6 -6 2 3.25 0.74-6-6 2 2.75 0.55-6 -6 1 0.98 0.39-6 -6 1 -0.15 0.47-6 -6 0 23.63 0.95-6 -6 0 23.77 1.62-6 -6 -1 24.95 1.02-6 -6 -1 25.83 1.69-6 -6 -2 22.69 1.39-6 -6 -2 22.32 1.58-6 -6 -3 19.87 1.30-6 -6 -3 17.93 1.03-6 -6 -4 -0.21 0.60-6 -6 -4 -0.09 0.44-6 -6 -5 9.08 0.70-6 -6 -5 7.47 0.79-6 -6 -6 15.31 0.83-6 -6 -6 16.64 1.42-6 -6 -7 0.68 0.43-6 -6 -7 0.85 0.80-6 -6 -8 0.35 0.37-6 -6 -8 0.23 0.72-6 -6 -9 9.39 0.97-6 -6 -9 7.63 1.17-6-7 5 1.87 0.70-6 -7 5 2.19 0.73-6 -7 4 22.31 1.31-6 -7 4 21.29 1.00-6 -7 3 0.38 0.50-6 -7 3 -0.44 0.53-6 -7 2 0.18 0.40-6 -7 2 1.57 0.71-6 -7 1 3.88 0.86-6 -7 1 5.06 0.97-6 -7 0 2.08 0.75-6-7 0 1.81 0.86-6 -7 -1 0.55 0.65-6 -7 -1 0.50 0.50-6 -7 -2 4.36 0.91-6-7-2 5.16 1.08-6 -7 -3 0.18 0.41-6 -7 -3 0.33 0.76-6 -7 -4 -0.26 0.67-6 -7 -4 0.82 0.51-6 -7 -5 5.58 0.96-6 -7 -5 4.81 0.74-6 -7 -6 14.88 0.90-6 -7 -6 18.66 1.54-6 -7 -7 0.42 0.43-6 -7 -7 -0.04 0.76-6 -7 -7 0.39 0.78-6 -7 -8 0.22 0.35-6 -7 -8 -0.27 0.42-6 -7 -9 7.91 1.04-6 -7 -9 8.55 1.14-6 -8 4 2.92 0.80-6 -8 4 2.75 0.85-6 -8 3 0.40 0.59-6 -8 3 0.06 0.41-6 -8 2 1.55 0.48-6 -8 2 2.52 0.83-6 -8 1 1.25 0.73-6 -8 1 1.57 0.86-6 -8 0 0.13 0.60-6 -8 0 0.26 0.47-6 -8 -1 1.91 0.78-6 -8 -1 2.81 1.00-6 -8 -2 0.81 0.75-6 -8 -2 2.07 0.91-6 -8 -3 3.25 0.87-6 -8 -3 4.11 1.07-6 -8 -4 5.50 0.64-6 -8 -4 5.90 1.15-6 -8 -5 -0.55 0.67-6 -8 -5 -0.25 0.50-6 -8 -6 7.07 1.06-6 -8 -6 7.03 1.22-6-8-7 7.18 1.07-6 -8 -7 6.08 1.19-6 -8 -8 13.51 1.27-6 -8 -8 10.94 1.39-6 -8 -9 19.70 1.51-6 -8 -9 20.80 1.64-6 -9 2 4.46 0.62-6 -9 2 5.05 0.68-6 -9 1 5.63 1.00-6 -9 1 6.07 0.73-6 -9 0 6.79 1.04-6 -9 0 6.54 0.81-6 -9 -1 4.77 1.00-6 -9 -1 6.29 1.20-6 -9 -2 4.70 1.02-6 -9 -2 6.34 0.78-6 -9 -3 0.47 0.71-6 -9 -3 0.14 0.85-6 -9 -4 6.27 0.72-6 -9 -4 8.31 1.35-6 -9 -5 7.50 1.13-6 -9 -5 8.29 0.91-6 -9 -6 4.44 0.67-6-9-6 5.61 0.82-6 -9 -7 4.36 1.04-6 -9 -7 4.77 1.17-6 -9 -8 1.20 0.88-6 -9 -8 3.00 0.97-6 -10 0 5.06 1.02-6 -10 0 4.21 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0.45-8 -5 3 0.43 0.51-8 -5 2 -0.11 0.79-8 -5 2 1.14 0.61-8 -5 1 0.80 0.79-8 -5 0 1.28 0.88-8 -5 -1 0.13 0.77-8 -5 -2 0.56 0.85-8 -5 -3 5.85 0.80-8 -5 -4 1.40 0.95-8 -5 -5 1.16 0.89-8 -6 2 18.63 1.46-8 -6 2 17.31 1.78-8 -6 1 2.35 0.60-8 -6 1 2.81 1.16-8 -6 0 2.43 0.62-8 -6 0 2.34 1.17-8 -6 -1 1.20 0.57-8 -6 -1 0.46 1.12-8-6-2 0.89 0.79-8 -6 -2 -0.17 0.66-8 -6 -3 1.04 0.84-8 -6 -3 0.04 0.70-8 -6 -4 6.38 0.82-8 -6 -4 7.86 1.05-8 -6 -5 11.03 1.42-8 -6 -5 11.57 1.16-8 -7 0 17.80 1.58-8 -7 0 16.79 1.89-8 -7 -1 5.48 1.17-8 -7 -1 5.22 1.47-8 -7 -2 5.99 0.83-8 -7 -2 5.61 0.98-8 -7 -3 1.90 1.04-8 -7 -3 1.62 1.24-8 -7 -4 14.73 1.910 0 0 0.00 0.00;_shelx _hkl校验和17337_shelx文件;标题SH177货架.res由SHELXL-2019/2于2022年10月22日20:49:55创建手机0.71075 6.67339 9.80442 10.51565 65.80390 89.89400 74.73630零1 0.00049 0.00076 0.00070 0.00460 0.00630 0.00530LATT 1号机组SFAC公司总部单元26 34 6省略-3-4 6L.S.10号机组飞行管理计划2平面图10HTAB公司债券$H形态温度-100.0ACTA公司尺寸0.290 0.210 0.060WGHT 0.084500 0.088100自由值0.68979O1 3 0.500778 0.616985 0.266865 11.000000.04085 0.04953=0.03159 -0.01634 0.01016 -0.02755氧气3-0.155210 0.271175 0.202882 11.000000.04790 0.05884=0.03907 -0.02365 0.00446 -0.02883臭氧层3-0.130068 0.214685 0.432895 11.00000 0.03623 0.04334=0.03892 -0.01702 0.00731 -0.02281C1 1 0.955741 0.952718 0.064711 11.000000.03414 0.03476=0.03574 -0.01412 0.00604 -0.01558AFIX第23页H1A 2 0.875445 1.023516 0.104138 11.00000-1.20000H1B 2 1.073077 0.875112 0.136554 11.00000-1.20000AFIX 0公司C2 1 0.813570 0.867532 0.034674 11.00000 0.03215 0.03454=0.03540 -0.01359 0.00628 -0.01593AFIX第23页H2A 2 0.696733 0.944785-0.037757 11.00000-1.20000H2B 2 0.894056 0.795510-0.003499 11.00000-1.20000AFIX 0公司C3 1 0.724576 0.775054 0.165057 11.000000.03388 0.03609=0.03422 -0.01372 0.00595 -0.01517AFIX第23页H3A 2 0.841692 0.697379 0.237046 11.00000-1.20000H3B 2 0.645698 0.847111 0.203703 11.00000-1.20000AFIX 0公司C4 1 0.582042 0.691397 0.137024 11.000000.03268 0.03694=0.03304 -0.01229 0.00809 -0.01758AFIX第23页H4A 2 0.466187 0.766566 0.062869 11.00000-1.20000H4B 2 0.660781 0.612463 0.105526 11.00000-1.20000AFIX 0公司C5 1 0.363218 0.536013 0.268678 11.00000 0.02742 0.03241=0.03232 -0.01278 0.00226 -0.01056C6 1 0.300872 0.512304 0.154506 11.000000.03581 0.03945=0.02801 -0.01346 0.00744 -0.01513AFIX第43页H6 2 0.354087 0.554669 0.067383 11.00000-1.20000AFIX 0公司C7 1 0.160396 0.426208 0.169810 11.000000.03303 0.03941=0.03344 -0.01805 0.00220 -0.01234AFIX第43页H7 2 0.118981 0.409221 0.092424 11.00000-1.20000AFIX 0公司C8 1 0.078638 0.364091 0.295876 11.00000 0.02726 0.03034=0.03353 -0.01343 0.00211 -0.00963C9 1 0.142435 0.388318 0.409805 11.000000.03088 0.03769=0.02909 -0.01313 0.00609 -0.01456AFIX第43页H9 2 0.088819 0.346062 0.496787 11.00000-1.20000AFIX 0公司C10 1 0.282596 0.473146 0.396382 11.000000.03315 0.04377=0.02998 -0.01713 0.00376 -0.01667AFIX第43页H10 2 0.324872 0.489132 0.474169 11.00000-1.20000AFIX 0公司C11 1-0.079361 0.280247 0.302581 11.000000.02974 0.03221=0.03797 -0.01589 0.00387 -0.00952C12 1-0.282617 0.127523 0.451252 11.000000.03314 0.03882=0.04660 -0.01965 0.00711 -0.01865AFIX第23页H12A 2-0.225921 0.035401 0.431134 11.00000-1.20000H12B 2-0.413088 0.194284 0.387294 11.00000-1.20000AFIX 0公司C13 1-0.324389 0.077329 0.602030 11.000000.04578 0.04899=0.05037 -0.02234 0.01603 -0.02596AFIX 137型H13A 2-0.423756 0.015410 0.620866 11.00000-1.20000H13B 2-0.383525 0.169814 0.619571 11.00000-1.20000H13C 2-0.193089 0.014077 0.663841 11.00000-1.20000AFIX 0公司HKLF 4号机组REM SH177型所有数据的REM wR2=0.1637,GooF=S=1.101,受限GooF=1.101REM R1=0.0578(对于2065 Fo>4sig(Fo))和0.0750(对于所有2739数据)使用0约束优化REM 146参数结束WGHT 0.0845 0.0881REM潜在氢键说明EQIV$2-x+1,-y+1,-z+1HTAB C10 O1_ 2美元REM最高差值峰值0.479,最深孔-0.256,1σ水平0.057第一季度0.6477 0.7428 0.1441 11.00000 0.05 0.48第2季度-0.0041 0.3317 0.2963 11.00000 0.05 0.47问题3 1 0.4261 0.5875 0.2641 11.00000 0.05 0.42问题4 1 0.3266 0.5290 0.2250 11.00000 0.05 0.38问题5 1 0.8766 0.9150 0.0424 11.00000 0.05 0.38问题6 1 0.2072 0.4404 0.3989 11.00000 0.05 0.35问题7 1-0.2128 0.1708 0.4375 11.00000 0.05 0.33问题8 1 0.2019 0.4910 0.1622 11.00000 0.05 0.32问题9 1 0.1045 0.3800 0.3466 11.00000 0.05 0.30问题10 1 0.3375 0.5098 0.3286 11.00000 0.05 0.28;_搁置_校验和94179